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KMID : 1059520070510040346
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Journal of the Korean Chemical Society
2007 Volume.51 No. 4 p.346 ~ p.351
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Dry Media Reaction Procedure for Synthesis of α,β-Unsaturated Acids, α-Cyanoacrylonitriles and α-Cyanoacrylates via Knoevenagel Condensation Using NaHSO4·SiO2 Catalyst
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M. Gopalakrishnan
P. Sureshkumar
J. Thanusu
S. Thirunavukkarasu
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Abstract
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Efficient stereoselective synthesis of α,β-Unsaturated acids, α-Cyanoacrylonitriles and α-Cyanoacrylates has been carried out in the presence of NaHSO4·SiO2 under solvent?free conditions with an E-geometry.
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KEYWORD
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NaHSO4·SiO2, (E)-3-(2-butyl-4-chloro- 1H-imidazol-5-yl)acrylic acid, Microwave irradiation , Silica Gel Supported Sodium Hydrogen Sulphate, Knoevenagel Condensation, Aryli
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